常量重量法测定有机锡锡含量的研究  

Analysis of Tin Content in Organotin Compounds by Gravimetric Method

作　　者：贺庆林[1] 包明[1] 刘继红[1] 刘宝殿 

机构地区：[1]东北师范大学化学系

出　　处：《东北师大学报（自然科学版）》1996年第1期61-63,共3页Journal of Northeast Normal University(Natural Science Edition)

基　　金：吉林省科学技术委员会应用基础资助

摘　　要：运用常量重量法测定了有机锡化合物锡的含量，确定了分析条件和过程．对不同类型有机锡化合物含量的分析结果表明，该方法易于操作，简便快速，结果准确，重现性好．The gravimetric method was studied for the analysis of tin content in organotic compounds, Analytic conditions and process were carefully investigated. 0. 1000-0. 20009 of sample was decomposed with 2-3 drops of concentrated H2SO4 and HNO3(Volume 1: 1), The excessive acid was evapovated directly on a low flame, the residuewas ignited at 900℃ for 2h, finally formed is SnO2 and weighed. The adventage of thedeveloped method are simple, rapid high accuracy and good reproducibity.

关 键 词：锡 有机锡化合物 重量分析法 测定 

分 类 号：O627.42[理学—有机化学]