棒状纳米PbO的固相合成  

Solid State Synthesis of PbO Nanorods

作　　者：高艳阳[1] 张月[1] 王金霞[1] 

机构地区：[1]中北大学化工与环境学院,山西太原030051

出　　处：《中北大学学报（自然科学版）》2007年第1期57-59,共3页Journal of North University of China(Natural Science Edition)

摘　　要：分别以Pb(Ac)2.3H2O、Pb(NO3)2为原料,与NaOH在室温条件下进行固相化学反应,得到了纳米PbO粒子.通过在反应体系中添加NaCl,成功地制得了棒状PbO纳米粒子.运用X射线衍射(X-Ray Diffractomer,XRD)和透射电镜(Transmission Electron Microscope,TEM)对产物进行了表征.研究表明,氯离子的存在对产物PbO的形貌有很大影响.Nanometer PbO were prepared by solid state reaction at room temperature via sodium hydroxide and lead acetate or lead nitrate, and PbO Nanorods were successfully prepared in the presence of sodium chloride. The productions were characterized by X-ray Diffractomer （XRD） and Transmission Electron Microscope （TEM）. The result indicates that the chloride ion has much influence on the formation of PbO nanorods.

关 键 词：纳米 棒状 氧化铅 固相合成 

分 类 号：O614.43[理学—无机化学]