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作 者:胡永美[1] 杜彰礼[1] 汪豪[1] 叶文才[1] 赵守训[1]
机构地区:[1]中国药科大学天然药化教研室,江苏南京210009
出 处:《中国中药杂志》2007年第7期603-605,共3页China Journal of Chinese Materia Medica
摘 要:目的:对芝麻花Sesamum indicum的化学成分进行研究。方法:运用硅胶柱色谱、凝胶柱色谱、反相柱色谱等多种色谱手段进行分离纯化,根据理化性质和波谱数据鉴定化合物的结构。结果:共得到6个黄酮类化合物,分别鉴定为芹菜素(1),鼬瓣花亭(ladanetin,2),鼬瓣花亭-6-O-β-D-葡萄糖苷(ladanetin-6-O-β-Dglucoside,3),芹菜素-7-O-葡糖醛酸(ap igen in-7-O-glucuron ic ac id,4),胡麻素(pedalitin,5),胡麻素-6-O-葡萄糖甙(pedalitin-6-O-glu-coside,6)。结论:6个黄酮化合物均为首次从该植物中分离得到。Objective: To investigate the chemical constituents from flowers of Sesamurn indicum. Method: Column chromatography with silica gel, C18 and Sephadex LH -20 as packing materials was used to separate the chemical constituents, and the structures were determined by chemical and spectroscopic methods. Result: Six flavones were isolated and elucidated as apigenin (1), ladanetin (2), ladanetin-6-O-β-D-glucoside (3), apigenin-7-O-glucuronic acid (4), pedalitin (5), and pedalitin-6-O-glucoside (6). Conclusion: All of the compounds were isolated from this plant for the first time.
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