Synthesis and Purification of Porphyrin-Schiff Base Using Ethyl Vanillin  

作　　者：WANG Dong SU Lian-jiang CHENG Xiu-li SUN Er-jun SHI Tong-shun 

机构地区：[1]College of Chemistry, Jilin University, Changchun l30021, P. R. China [2]Department of Chemistry, Daqing Teachers College, Daqing 163712, P. R. China

出　　处：《Chemical Research in Chinese Universities》2007年第2期135-137,共3页高等学校化学研究（英文版）

基　　金：the National Natural Science Foundation of China(No 59783001)

摘　　要：A novel porphyrin-Schiff base was synthesized via the condensation of 5-（4-aminophenyl） -10,15,20-triphenylperphyrin and ethyl vanillin. After analyzing the level of purification of the perphyrin-Schiff base, it was successfully separated. This perphyrin-Schiff base was characterized by using UV-Vis, IR,^1H NMR and MS spectroscopy.A novel porphyrin-Schiff base was synthesized via the condensation of 5-（4-aminophenyl） -10,15,20-triphenylperphyrin and ethyl vanillin. After analyzing the level of purification of the perphyrin-Schiff base, it was successfully separated. This perphyrin-Schiff base was characterized by using UV-Vis, IR,^1H NMR and MS spectroscopy.

关 键 词：SYNTHESIS Porphyrin-Schiff base Ethyl vanillin PURIFICATION 

分 类 号：O625.632[理学—有机化学]