溶剂解析气相色谱法测定室内空气中的苯和苯系物  被引量:11

Benzene and benzene series in the room air was estimated by solvent relief absorption gas chromatography

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作  者:周建钟[1] 周钰芳[2] 任媛媛[3] 高兴军[1] 肖继波[3] 

机构地区:[1]浙江林学院理学院,浙江临安311300 [2]丽水学院医学部,浙江丽水323000 [3]浙江林学院环境科技学院,浙江临安311300

出  处:《湖南理工学院学报(自然科学版)》2007年第2期57-60,共4页Journal of Hunan Institute of Science and Technology(Natural Sciences)

基  金:浙江林学院高等教育研究重大招标项目(0406);浙江林学院科学研究发展基金资助项目(235100021)

摘  要:采用气相色谱法测定室内空气中的苯和苯系物。方法:采用活性炭管采集,经二硫化碳解析,HP-5石英毛细管柱作为分离柱,FID检测器,考察了苯及苯系物的线性、计算因子。结果:以峰面积为基础,线性回归情况良好,可以较准确的定量;苯、甲苯、乙苯、间(对)二甲苯、邻二甲苯的计算因子分别为6.266×10-4、6.527×10-4、6.647×10-4、5.599×10-4、7.120×10-4。对浙江林学院学生宿舍、食堂、餐厅、超市进行了测定。结果表明:上述场所苯浓度均小于0.09mg/m3,苯系物浓度总和小于0.9 mg/m3。Using solvent relief absorption gas Chromatography to estimate the concentration of the Benzene and benzene series in the room air. The method: It adopted the active carbon tube to collect samples, which were relieved by CS2 absorption with HP-5 capillary gas chromatography and FID detector. It studied the linearity and calculation factors of the benzene and the benzene series. Results: Regarding peak area as the foundation, linear regression turned all right, it can be accurate fixed the amounts; the benzene, toluene, ethyl benzene, (m,p)-xylene, o-xylene calculation factors respectively for 6.266×10^-4, 6.527×10^-4, 6.647×10^-4, 5.599×10^-4. 7.120×10^-4. From the students dormitories, dining rooms, restaurants, super markets for Zhejiang forestry University proceeds measurement, results showed that in the above places the benzene concentration measured were all less than 0.09mg/m^3, the total concentration of benzene series is far less 0.9mg/m^3.

关 键 词:气相色谱 室内空气  苯系物 

分 类 号:O657.71[理学—分析化学] O623[理学—化学]

 

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