HPLC测定蔬菜、水果中氨基甲酸酯类农药残留量  

Measurements of Carbamate Pesticides Residual Quantity in Vegetable and Fruit by Using HPLC

作　　者：张静[1] 闫实[2] 王蕾[1] 王宁[3] 

机构地区：[1]沈阳化工学院理化测试中心,辽宁沈阳110142 [2]农业部农业环境质量监督检验测试中心,辽宁沈阳110034 [3]东北大学研究设计院(有限公司),辽宁沈阳110013

出　　处：《沈阳化工学院学报》2007年第2期156-160,共5页Journal of Shenyang Institute of Chemical Technolgy

摘　　要：采用高效液相色谱（配荧光检测器和柱后衍生系统）测定菜豆、油菜、苹果中涕灭威亚砜、涕灭威砜、三羟基克百威、涕灭威、速灭威、克百威、西维因、异丙威、仲丁威9种氨基甲酸酯类农药的残留量,对每种农药做3种不同浓度（0.05、0.100、.50 mg·kg^-1）添加回收率实验.结果表明：该方法对9种农药的回收率为74%-114%,变异系数在15%之内,最小检出限为0.001 0-0.007 5mg·kg^-1.A rapid, simple analysis method for determining residues of Aldicarb sulfoxide, Aldicarb sullone, 3-Hydroxycarbofuran, Aldicarb, Mctolcarb, Carbofuran, Carbaryl, Ispricarb, BPMC in bean, cole and apple by the high performance liquid chromatography was studied. All pesticides were added with three kinds of contents （0.05,0.1,0.5 mg·kg^-1） in the recovery experiment. The average recoveries of the analytical method for the fortified samples in bean cole and apple were 74 %-114 %, with the coefficient of variation within 15 %. The minimum detection limits for nine kinds of carbamate pesticides were in range of 0.001 0-0.007 5 mg·kg^-1.

关 键 词：高效液相色谱 氨基甲酸酯 残留量 

分 类 号：O657.72[理学—分析化学]