一种新型气相色谱固定液的制备及应用  

Study and Apply of a New GC Stationary Liquid

作　　者：张丽嫒[1] 陈天舒 申书昌[3] 王文波[3] 

机构地区：[1]黑龙江八一农垦大学食品学院,黑龙江大庆163319 [2]齐齐哈尔市建华区卫生防疫站,黑龙江齐齐哈尔161006 [3]齐齐哈尔大学化学与化学工程学院,黑龙江齐齐哈尔161006

出　　处：《化工时刊》2007年第6期44-46,共3页Chemical Industry Times

基　　金：黑龙江省教育厅科学技术研究项目(11511437)

摘　　要：以柠檬酸、OP-10和二乙醇胺为原料合成了柠檬酸壬基酚聚氧乙烯醚单酯二乙醇酰胺。用红外光谱法表征了结构,热分析技术考察了热稳定性。以此产物作为气相色谱固定液,对一些混和组分进行分离,效果良好。The citric acid polyethyleneoxide ether amber diehylene glycol dinitrate diglycollic amid was synthesized by the citric acid and the polyoxyethylene nonyl phenyl ether and the diethanolamine. The structure of the product was determined by IR spectrum. The thermal stability was investigated via thermogravimetry analysis（TG）. The surfactants could be used as gas chromatographic stationary liquid, the good behavior of the stationary liquid was showed by separation efficiency to some component in mixture samples.

关 键 词：柠檬酸壬基酚聚氧乙烯醚单酯二乙醇酰胺 合成 气相色谱固定液 

分 类 号：O657.71[理学—分析化学]