二甘氨酸合锌(Ⅱ)配合物的制备  

THE PREPARATION OF A COORDINATION COMPOUND OF BISGLYCINATO ZINC (Ⅱ) MONOHYDRATE

作　　者：骆鑫[1] 祝晓元[1] 徐小平[1] 窦后松[1] 方震乾[2] 谢益农[2] 

机构地区：[1]华西医科大学药学院,成都610041 [2]四川联合大学化工学院,成都610065

出　　处：《华西药学杂志》1997年第1期17-18,共2页West China Journal of Pharmaceutical Sciences

摘　　要：制备了二甘氨酸含锌（Ⅱ）配合物，并用化学法进行了鉴定，配位滴定法进行了含量测定，用热谱确定了配合物含一分子结晶水，在281℃熔化时分解，经元素分析和红外光谱确定了结构。A coordination compound of bisglycinato zinc (Ⅱ ) monohydrate was prepared by thegeneral synthesis method. The product samples were identified by chemical method. The content was analysed by compleximetry. The result showed that zinc is 98. 8%. The thermal analysis showed that it contains one molecule of crystal water and it decomposes when melting at 281℃. Its structure was elucidated on the basis of infra-red studies as well as elementary analysis.

关 键 词：甘氨酸合锌 配合物 制备 

分 类 号：TQ463.6[化学工程—制药化工]