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机构地区:[1]南昌大学理学院化学系,江西南昌330006 [2]南昌大学药学系,江西南昌330026
出 处:《中国现代中药》2007年第8期15-16,19,共3页Modern Chinese Medicine
摘 要:目的:建立陆英颗粒的质量标准。方法:采用薄层色谱法鉴别熊果酸,并应用UV测定以芦丁计总黄酮的含量。结果:TLC法专属性强,含量测定以芦丁计总黄酮在0.008~0.065mg.mL-1呈良好的线性关系,平均回收率为98.58%,RSD=0.34%。结论:本质量标准可有效地控制陆英颗粒的质量,且方法稳定、简便可行。To establish the quality standard of Sambucus chinensis Lindl. granules. Methods: TLC was used for simultaneous identification of arsolic acid , UV was used for the determination of all flavonoids depending on rutin. Results: The TLC identification was highly specific and the spots was clear. The linearity for all flavonoids depending on rutin was obtained over the range of 0. 008 - 0. 065rag. mL^- l. The average recovery of rutin was 98.58%, RSD = 0. 34%. Conclusion: This quality standard was capable of effectively controlling the quality of Sambucus chinensis Lindl. granules. The method is simple quick accurate and the result of determination is good.
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