补血糖浆的质量标准  

Quality standard for Buxue Syrup

作　　者：贺国芳[1] 林芳[1] 闵敏[1] 魏世超[1] 方慕初[1] 

机构地区：[1]华中科技大学同济医学院附属同济医院药学部

出　　处：《中国药师》2007年第10期980-981,共2页China Pharmacist

摘　　要：目的:制定补血糖浆的质量标准。方法:采用薄层色谱(TLC)法对处方中鸡血藤、虎杖进行定性鉴别;采用高效液相色谱法测定补血糖浆中大黄素的含量。结果:TLC鉴别方法专属性强,大黄素在4.6～46.2μg·ml^(-1)浓度范围内与峰面积线性关系良好,r=0.999 9,平均回收率为99.2%,RSD=1.2%(n=6)。结论:本质量标准可有效控制补血糖浆的质量。Objective： To establish the quality standard for buxue syrup. Method： Spatholobus suberectus dunn（SSD） and Rhizoma ET Radix polygoni cuspidati were identified by TLC, the emodin was determined by HPLC. Result： SSD and Rhizoma polygoni cuspidati could be identified by TLC, the linear range of emodion was 4.6 - 46.2 μg·ml^-1（ r = 0.999 9 ）, the average recovery was 99.2% with RSD 1.2% （ n = 6）. Conclusion： The method is accurate and reproducible, it can be used for quality control of Buxue syrup.

关 键 词：补血糖浆 质量标准 薄层色谱 高效液相色谱 大黄素 

分 类 号：TQ460.72[医药卫生—药物分析学]