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机构地区:[1]大庆石油学院化学化工学院,黑龙江大庆163318
出 处:《中山大学学报(自然科学版)》2007年第B06期248-249,共2页Acta Scientiarum Naturalium Universitatis Sunyatseni
基 金:黑龙江省教育厅科学技术研究项目资助(10551006)
摘 要:以马来酸酐为原料制备聚天冬氨酸,并对聚合反应的质量配比、聚合温度和聚合时间三个反应条件进行了优化实验,对最优条件下合成的PASP与其它阻垢剂进行了性能对比。结果表明:合成PASP的最佳条件是:原料质量配比为1∶1.1,聚合温度为160℃,聚合时间为1h,阻垢率可以达到95%以上,生物降解性能达到70%。Polyaspartic acid (PASP) was prepared by the means of polymerizing maleic anhydride and ammonia solution. In order to find optimal condition of synthesizing PASP, we made a set of experiments on proportion of material, temperature and time of polymeri- zation in the single condition, and compared PASP with other scale inhibitors about the performance of scale inhibition and biodegradation . The results show : the optimal proportion of material is 1 : 1.1, the temperature of polymerization is 160℃, and the time of polymerization is l h. Under above condition, we synthetized the PASP its inhibiting efficiency can reach over 95%, and biodegradation rate reaches 70%.
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