磨浆-超声法提取黄姜中薯蓣皂苷元的工艺研究  

Process of extracting diosgenin from Dioscorea zingiberensis by grinding starch and ultrasonic extracting method

作　　者：李冬[1] 李稳宏[1] 韩枫[1] 廉媛 陈练洪[1] 唐璇 

机构地区：[1]西北大学陕西省资源化工应用工程技术研究中心/化工学院,陕西西安710069 [2]陕西地矿医院,陕西西安710014

出　　处：《中草药》2007年第12期1815-1817,共3页Chinese Traditional and Herbal Drugs

基　　金：陕西省科技厅重点攻关项目(04K09-G15);陕西省教育厅重大产业化项目(04JC03);西安市科技局工业攻关项目(GG05083)

摘　　要：目的优化磨浆-超声法从黄姜中提取薯蓣皂苷元工艺条件。方法采用对黄姜磨浆预处理后超声提取,再进行酸水解的方法从黄姜中提取薯蓣皂苷元。结果通过正交试验得到提取过程优化的工艺条件:磨浆时间5min,超声时间50min;料液比1∶18g/mL。其中料液比和磨浆时间对提取过程影响显著。与传统的直接酸水解法相比,收率提高了18%。结论磨浆-超声法用于黄姜提取具有收率高、污染少、节约能源的特点。Objective To optimize the experiment conditions in process for extracting diosgenin from Dioscorea zingiberensis. Methods A new method of grinding starch pretreatment, ultrasonic extracting, and hydrochloric acid hydrolyzing was studied. Results The optimal experiment condition was obtained, grinding starch 5 min, ultrasonic extraction 50 min, the ratio of material and solvent was 1 ： 18. The ratio of the material and solvent had the greatest effect to the extraction process. Its extraction percentage had been raised 18% compared with the traditional method. Conclusion The method has the characteristics of energy-saving with high yield and low pollution.

关 键 词：黄姜 薯蓣皂苷元 磨浆 超声提取 

分 类 号：R286.1[医药卫生—中药学]