SYNTHESIS AND CHARACTERIZATION OF N-(1-NAPHTHYL) SUCCINIMIDE  

SYNTHESIS AND CHARACTERIZATION OF N-(1-NAPHTHYL) SUCCINIMIDE

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作  者:LI Hexian YANG Hailong LIU Kun WANG Ying YUAN Jialong WANG Guochang 

机构地区:[1]Institute of Polymer Chemistry, Nankai University, Tianjin 300071, China

出  处:《Chinese Journal of Reactive Polymers》2007年第1期1-6,共6页中国反应性高分子(英文版)

基  金:Natural Science Foundation of China (50273014, 29928003);Natural Science Foundation of Tianjin (03380261).

摘  要:In this paper a modified two-step procedure for synthesis of N-(1-naphthyl) suecinimide (NaS) was developed, and the molecular structure of NaS was properly characterized by XRD, FT-IR, 1H NMR, DSC, etc. The results show that the melting point of our product is 159 ℃-160.5 ℃, and the characteristic infrared absorption band of carbonyl group splits into two peaks (1705cm^-3/1779cm^-3), which are found to be quite different from the documented data (rap 147℃ -149℃; IR C=0-1700cm^-3). Besides, photophysical spectroscopy was found to be powerful to study the molecular structure and crystal morphology of NaS compound.

关 键 词:N-(1-naphthyl) succinimide MICROCRYSTALS lnfrared spectrum Fluorescence spectra. 

分 类 号:O631[理学—高分子化学]

 

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