微波无溶剂法合成香草醛氨基酸席夫碱  

Microwave-assisted solvent-free synthesis of schiff base from vanillin and amino acid

作　　者：李建平[1] 吉彦[1] 刘锐杰[1] 张永霞[2] 

机构地区：[1]河南师范大学化学与环境科学学院；河南新乡453007 [2]河南师范大学河南省环境污染控制重点实验室,河南新乡453007

出　　处：《化学研究与应用》2008年第1期87-89,共3页Chemical Research and Application

基　　金：河南省自然科学基金资助项目(0611021700);河南省教育厅自然科学基金资助项目(2007150024)

摘　　要：In this study,a number of amino acid schiff bases from vanillin and amino acid have been synthesized under microwave irradiation coupled with solvent-free condition,which proves to be simple and efficient.The structure of the prepared compounds are characterized by elemental analysis,IR,1H NMR and electronic spectra.In this study, a number of amino acid schiff bases from vanillin and amino acid have been synthesized under microwave irradiation coupled with solvent-free condition, which proves to be simple and efficient. The structure of the prepared compounds are characterized by elemental analysis ,IR, ^1 H NMR and electronic spectra.

关 键 词：氨基酸席夫碱 微波辐射 无溶剂反应 合成 

分 类 号：O621.3[理学—有机化学]