2,2′-(1,4-乙二氧基)-二苯甲酸甲酯及其羟肟酸的合成  

Synthesis and characterization of 2,2′ (1,4 ethylenedioxy) methyl dibenzoate and 2,2′ (1,4 ethylenedio xy) dibenzhydroxamic acid

作　　者：王世范[1] 赵亮[1] 谢复新[1] 赵祥大[1] 倪诗圣[1] 

机构地区：[1]安徽大学化学系

出　　处：《化学试剂》1997年第4期235-236,244,共3页Chemical Reagents

基　　金：国家自然科学基金

摘　　要：以水杨醛、１，２－二溴乙烷、ＳＯＣｌ２等为原料合成了两种新型的开链聚醚，并对它们进行了红外光谱、元素分析、核磁、质谱表征。The synthesis and characterization of two kinds of new open chain polyether are reported By the reaction of 2,2′ (1,4 ethylenedioxy) dibenzene carboxylic acid with SOCl 2,we first synthesized 2,2′ (1,4 ethylenedioxy) dibenzoyl chloride and then prepared 2,2′ (1,4 ethylenedioxy) methyl dibenzoate and 2,2′ (1,4 ethylenedioxy) dibenzhydroxamic acid by the acylation of 2,2′ (1,4 ethylenedioxy) dibenzoyl chloride They were characterized by IR, 1HNMR,MS and elemental analysis

关 键 词：水杨醛 聚醚 螯合剂 羟肟酸 二苯甲酸甲酯 

分 类 号：O641.4[理学—物理化学]