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机构地区:[1]浙江省医学科学院,杭州310013
出 处:《天然产物研究与开发》2007年第B05期117-118,136,共3页Natural Product Research and Development
摘 要:测定保健食品中红景天甙的含量以控制产品质量。采用十八烷基硅烷键合硅胶柱;以乙腈-水(1:9)为流动相,流速为1.0mL/min,检测波长为280nm。结果表明红景天甙在0.4—4.0μg范围内呈线性关系,平均回收率(n=6)为98.96%(RSD=1.16%)。该方法简便、准确、重现性好,可用于保健食品中红景天甙的质量控制。To determine salidroside in health food for establishing a method of quality control, an ODS colunm was used with a mobile phase consisted of mixture of acetonitrile-water buffer( 1: 9) ,flow rate was 1.0 mL/min, and detector wavelength was 280 nm. The linear range of salidroside was 0.4- 4.0 μg. The average recovery was 98.96% ( RSD = 1.16% ,n =6). The method appeared to be simple,accurate with good reproducibility,and can be used to the quality control.
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