脱氧胆酸裂口分子的微波合成  

Synthesis of Molecular Clefts Based on Deoxycholic Acid under Microwave Irradiation

作　　者：陈静[1] 赵志刚[1] 刘兴利[1] 石云[1] 

机构地区：[1]西南民族大学化学与环境保护工程学院,四川成都610041

出　　处：《合成化学》2008年第1期28-32,共5页Chinese Journal of Synthetic Chemistry

摘　　要：以固体K2CO3为载体,在微波辐射无溶剂条件下,脱氧胆酸甲酯与芳酰氯反应合成了9个新的脱氧胆酸裂口分子人工受体,其结构经1HNMR,IR,MS及元素分析表征。Nine new molecular clefts based on deoxycholic acid were synthesized by the reaction of methyl deoxycholate with aroyl chloride using solid K2CO3 as a supporter in solvent-free under microwave irradiation. The structures were characterized by ^1H NMR, IR, MS and elemental analysis.

关 键 词：脱氧胆酸 裂口分子 微波合成 分子识别 

分 类 号：O641.3[理学—物理化学]