含噻二唑杂环的1，8-萘酰亚胺衍生物的合成与表征  

Synthesis and characterization of the derivatives of 1,8-naphthalimides containing thiadiazole heterocycle

作　　者：张业[1] 覃雯[1] 刘贤贤[1] 

机构地区：[1]桂林师范高等专科学校化学与工程技术系

出　　处：《化学试剂》2008年第3期211-212,226,共3页Chemical Reagents

基　　金：国家自然科学基金资助项目(20362002,20762001)

摘　　要：以4-溴-1,8-萘酐为起始原料,通过硝化、亲电取代、氢化还原、关环和亚酰化反应,合成了目标产物3,4-[1,2,3]-噻二唑-N-丙基-1,8-萘酰亚胺和3,4-[1,2,3]-噻二唑-N-丁基-1,8-萘酰亚胺。Two new derivatives of naphthalimides 3,4-[ 1,2, 3 ]-thiadiazole-N-propyl-1,8-naphthalimide and 3,4-[ 1,2,3]- thiadiazole-N-butyl-1, 8-naphthalimide were synthesized via nitration, nucleophilic substitution, hydrogenation, cyclization and imidafion of 4-bromo-naphthalic anhydride. The two compounds were characterized by IR, 1HNMR and elemental analysis.

关 键 词：萘酰亚胺 噻二唑 杂环 合成 表征 

分 类 号：O626[理学—有机化学]