一锅法合成五溴苄基溴  

One Pot Synthesis of Pentabromobenzyl Bromide

作　　者：董树安[1] 章国贞[1] 

机构地区：[1]山东师范大学有机合成重点实验室

出　　处：《精细化工》1997年第3期35-36,共2页Fine Chemicals

摘　　要：首次由甲苯经催化溴化制得五溴甲苯，不经分离直接在引发剂作用下进行α位甲基溴化，合成了五溴苄基溴，并对反应条件及其影响因素进行了讨论。Toluene was brominated with catalyst into pentabromotoluene (PMT),the bromide product wasn't separated and after initator and some more solvent were added,the further bromination began,after several hours pentabromobenzyl bromide (PBB) could be gotten.The results and the reaction conditions of the synthesis were investigated and discussed.

关 键 词：五溴苄基溴 阻燃剂 一锅法 合成 

分 类 号：TQ124.51[化学工程—无机化工] TQ242