1，3-双-(3-N-乙酰基-2-芳基-1，3，4-噁唑啉-5-基)苯化合物的合成与表征  

Synthesis and characterization of 1,3-bis-(3-N-acetyl-2-aryl-1,3,4-oxadiazoline-5-yl) benzene derivatives

作　　者：龙德清[1] 李德江[2] 唐传球[1] 

机构地区：[1]郧阳师范高等专科学校化学系,湖北丹江口442700 [2]三峡大学化学与生命科学学院,湖北宜昌443002

出　　处：《化学试剂》2008年第5期370-372,共3页Chemical Reagents

基　　金：湖北省教育厅重点科学技术研究项目(2004D001)

摘　　要：以间苯二甲酸二甲酯为起始原料,设计合成了8个新型的1,3-双-(3-N-乙酰基-2-芳基-1,3,4-噁唑啉-5-基)苯化合物,其结构经元素分析、IR、1HNMR和MS表征,并对其质谱裂解途径进行了探讨。Eight novel 1,3-bis- （ 3- N- acetyl-2- aryl- 1,3,4-oxadiazoline-5-yl） benzene derivatives were designed and synthesized using dimethyl m-phthalate as the starting material. All synthesized compounds were confirmed by elemental analysis, IR, ^1HNMR and MS, and the fragmentation mechanism of MS spectra was discussed as well.

关 键 词：双酰腙 双噁唑啉 合成 表征 

分 类 号：O626[理学—有机化学]