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出 处:《陕西科技大学学报(自然科学版)》2008年第3期75-78,共4页Journal of Shaanxi University of Science & Technology
基 金:广东省科技攻关项目(2006B13301006)
摘 要:采用真空蒸发法在普通玻璃表面制备了VO2薄膜,研究了退火温度和掺杂对薄膜表面形貌、晶体结构、电学性能和光学性能的影响.结果表明:经400℃、420℃、450℃、500℃退火得到的VO2薄膜其表面形貌和晶体结构存在明显的差异,其中420℃退火后的薄膜结晶形态良好,主要成分是VO2,在65℃左右表现出明显的电阻突变,常温下在波长1700nm附近薄膜的光透过率达59.9%;在VO2薄膜中掺入W6+,相变温度有所降低,但掺杂使薄膜光透过率降低.The thin films of were prepared by vacuum evaporation method. The surface morphologies, crystal structure, resistance-temperature characteristic was studied. The results show that the phase transition temperature of VO2 thin films, which undergo heat treatment at 400 ℃, 420℃ ,450℃, and 500℃, surface morphologies, crystal structure has significant difference. Thin films annealed at 420℃, exhibit good crystalline states, it's main components is VO2, electrical resistance change significantly at about 65 ℃, it's transparency is 59.9% at 1 700 nm wavelength. Doping W^6+ can reduce phase transition temperature, but it leads to the reduction of optical transmittance.
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