当归芍药散活性部位DSS-A-N--30中1种新单萜苷  

A new monoterpene glycoside from active fraction (DSS-A-N-30) of Danggui Shaoyao San

作　　者：胡绪玮[1] 乔善义[2] 范海涛[2] 李辰[1] 刘国云[2] 马渊[2] 周文霞[2] 张永祥[2] 

机构地区：[1]沈阳药科大学,辽宁沈阳110016 [2]军事医学科学院毒物药物研究所,北京100850

出　　处：《中国中药杂志》2008年第12期1413-1415,共3页China Journal of Chinese Materia Medica

摘　　要：目的:对当归芍药散活性部位DSS-A-N-30的化学成分进行研究。方法:用大孔树脂柱色谱制备DSS- A-N-30,用硅胶和反相硅胶柱色谱分离各成分,用MS及NMR技术鉴定结构。结果:从DSS-A-N-30中分离得到了1个新单萜苷。结论:新化合物命名为4″-羟基白芍苷。Objective： To study the chemical constituents of an active fraction （DSS-A-N-30） from Danggui Shaoyao San. Method： DSS-A-N-30 was prepared by macroporous resin chromatography, the compound was isolated by column chromatography on silica gel and RP C- 18, the structure was elucidated by spectroscopic methods. Result： A new monoterpene glycoside was isolated and identified from DSS-A-N-30. Conclusion： The new monoterpene glycoside was identified as 4＂-hydroxyl-albiflorin.

关 键 词：当归芍药散 化学成分 4″-羟基白芍苷 

分 类 号：R284.1[医药卫生—中药学]