黄丹结肠透析液的质量标准  

Quality Standards for Huangdan Colon Dialysis Solution

作　　者：付秀娟[1] 翟红玲[2] 陈晓亮[1] 李馨[1] 杨帆[2] 

机构地区：[1]吉林大学第二医院,长春130041 [2]吉林大学药学院

出　　处：《中国药师》2008年第6期639-640,666,共3页China Pharmacist

摘　　要：目的:建立黄丹结肠透析液的质量标准。方法:用薄层色谱法对大黄、川芎、丹参进行定性鉴别,用高效液相色谱法测定制剂中大黄素的含量。结果:薄层色谱鉴定方法专属性强。大黄素平均回收率为98.6%,RSD为0.98%。结论:本法简便、准确、灵敏、重现性好,可用于该制剂的质量控制。Objective： To establish the quality standards of Huangdan colon dialysis solution. Method： Radix et Rhizoma Rhei, Rhizoma Chuanxiong, Radix et Rhizema Salviae Mihiorrhizae in this preparation were identified by TCL, and the content of emodin in this preparation was determined by HPLC. Result： The spots in the TLC were clear and distinguished well. The average recovery of emodin was 98.6%, RSD = 0.98%. Conclusion： The method is simple, accurate, sensitive and reproducible, it can be used for the quality control of this preparation.

关 键 词：黄丹结肠透析液 薄层色谱法 大黄素 高效液相色谱法 

分 类 号：TQ460.72[医药卫生—药物分析学]