草豆蔻化学成分研究  

Studies on Chemical Constituents of Alpinia katsumadai

作　　者：王秀芹[1] 杨孝江 李教社[3] 

机构地区：[1]广州市药品检验所,广东广州510160 [2]深圳市康哲药业有限公司,广东深圳518209 [3]西安交通大学医学院,陕西西安710061

出　　处：《中药材》2008年第6期853-855,共3页Journal of Chinese Medicinal Materials

摘　　要：目的:研究草豆蔻乙醇提物中的化学成分。方法:采用硅胶柱色谱法进行分离纯化,理化及光谱分析鉴定结构。结果:从草豆蔻乙醇提取物中分离得到了8个化合物,鉴定了其中7个化合物,分别为:1,7-双苯-5-羟基-4,6-庚烯-3-酮基(Ⅰ)、1,7-双苯-4,6-庚烯-3-酮基(Ⅱ)、松属素(Ⅲ)、小豆蔻明(Ⅳ)、山姜素(Ⅴ)和7,4′-二羟基-5-甲氧基二氢黄酮(Ⅵ)、β-谷甾醇(Ⅶ)。结论:化合物Ⅰ、Ⅱ和Ⅶ为首次从该植物果实中分离得到,其中化合物Ⅰ和Ⅱ为首次从该属植物中分得。Objective： To study the chemical constituents from the ethanolie extract of Alpinia katsumadai Hayata. Methods： The compounds were separated with the column chromatographic, and their structures were identified by chemical and spectroscopic methods. Results ： Eight compounds were isolated from the ethanol extract. On the basis of their physical and chemical properties and spectroscopic analysis, the structures of seven compounds were identified. They were 1,7-Diphenyl-5-hydroxy-4, 6-heptadien-3-one（ Ⅰ）, 1,7-Diphenyl-4, 6-heptadien-3-one （ Ⅱ ）, Pinoeemhrin （Ⅲ ）, Cardamomin （ Ⅳ）, Alpinetin （ Ⅴ）, 7,4＇-Dihydroxy-5-methoxy flavanones（Ⅵ） and 13-Sitosterol（ Ⅷ）, respectively. Conclusion： Compounds Ⅰ , Ⅱ and Ⅶ are separated from this plant for the first time. Compounds Ⅰ and Ⅱ are also obtained from this genus of Alpinetin for the first time.

关 键 词：草豆蔻 化学成分 

分 类 号：R284.1[医药卫生—中药学] R284.2[医药卫生—中医学]