氨基甲酸酯型石胆酸分子裂缝的微波合成  

Microwave assisted synthesis of carbamate-type molecular clefts derived from lithocholic acid

作　　者：赵志刚[1] 

机构地区：[1]西南民族大学化学与环境保护工程学院,四川成都610041

出　　处：《化学研究与应用》2008年第7期919-922,共4页Chemical Research and Application

基　　金：西南民族大学博士创新基金资助项目(08NBS002)

摘　　要：A series of new molecular clefts are synthesized in good yields by using lithocholic acid as spacer to bridge different aromatic amines via triphosgene under microwave irradiation.Their structures are characterized by 1H NMR,IR,MS spectra and elemental analysis.Compared with the conventional method,this method is simple,safe,rapid,efficient and eco-friendly.A series of new molecular clefts are synthesized in good yields by using lithocholic acid as spacer to bridge different aromatic amines via triphosgene under microwave irradiation. Their structures are characterized by ^1H NMR, IR, MS spectra and elemental analysis. Compared with the conventional method, this method is simple, safe, rapid, efficient and eco-friendly.

关 键 词：石胆酸 分子裂缝 合成 微波辐射 

分 类 号：O641.3[理学—物理化学]