双甲胺草磷·吡嘧磺隆复配制剂的液相色谱分析  

Analytical Method of H9201 and Pyrazosulfuron in Mixture Formulation By HPLC

作　　者：陆雪芳[1] 王志敏[1] 戴宝江[1] 

机构地区：[1]南通江山农药化工股份有限公司,江苏南通226006

出　　处：《精细化工中间体》2008年第4期66-67,70,共3页Fine Chemical Intermediates

基　　金：国家科技支撑计划资助项目(2006BAE01A04-05)

摘　　要：介绍了应用液相色谱法同时测定除草剂双甲胺草磷(H9201)与吡嘧磺隆复配制剂两种有效成分含量的测定方法;采用乙腈-0.1%酸性水为流动相、C18柱、紫外检测器。双甲胺草磷与吡嘧磺隆的RSD分别为0.28%和0.32%,方法的线性相关系数均为0.9999和0.9998,平均回收率分别为99.58%和99.65%。The analysis of H9201 and pyrazosulfuron in mixture formulation by HPLC with C18 column using acetonitrile ＋ water ＋ acid as mobile phase and UV detector was introduced in this paper. Linear regression coefficient for H9201 and pyrazosulfuron was 0.999 9 and 0.999 8, respectively. The average recovery for H9201 and pyrazosulfuron was 99.58% and 99.6%, and RSD 0.28% and 0.28%, respectively.

关 键 词：双甲胺草磷 吡嘧磺隆 液相色谱 

分 类 号：O657.72[理学—分析化学]