三种赤芍药和脏连丸中芍药甙的含量测定  

THE QUANTITATIVE DETERMINATION OF PAEONIFLORIN IN THREE KINDS OF PAEONIA LACTIFLORA PALL AND ZANGLIAN WAN

作　　者：李章万[1] 郭平[1] 刘三康[1] 杨胜华[1] 

机构地区：[1]华西医科大学药学院,成都610041

出　　处：《华西药学杂志》1990年第3期152-154,共3页West China Journal of Pharmaceutical Sciences

摘　　要：本文用高效液相色谱法测定了三种赤芍药和脏连丸中芍药甙的含量。用50%乙醇提取样品,超声振荡30分钟;ODS柱分离,甲醇—异丙醇—36%醋酸—水(25:2:2:71)为流动相,检测波长230nm测得四川剥皮赤芍、甘肃赤芍、吉林赤芍、脏连丸中,芍药甙平均含量分别为4.09、2.01、1.94和0.208%。The paeonifilorin in three Paeoni lactiflora Pall and Zang li- an wan was determinated by HPLC.Pae- oniflorin can be separated on ODS column with a mobile phase (MeOH: (CH_3)_2CH OH:36%HAC:H_2O=25:2:2:71) and detected at 230nm. The samples was treated by 50% MeOH in ultrasonator for 30 min. The average contents of paeoniflorin are res- pectively 4.09% (in Sichuan Bopi Paeonia 1.p.) 2.01% (in Gansu Paeonia 1.p.) , 1.94% (in Jilin Paeonba 1.Pl)and 0.208% (in Zanglian Wan) .

关 键 词：赤芍药 芍药甙 脏连丸 含量测定 

分 类 号：R284.1[医药卫生—中药学]