痛经丸的质量标准  

Quality Standard for Tongjing Pills

作　　者：赵彩云 

机构地区：[1]徐州药品检验所,江苏徐州221006

出　　处：《中国药师》2008年第10期1181-1182,共2页China Pharmacist

摘　　要：目的:建立痛经丸的质量标准。方法:采用薄层色谱法对方中的当归、吴茱萸进行鉴别,采用高效液相色谱法测定淫羊藿苷的含量。结果:在薄层色谱中斑点清晰;淫羊藿苷在0.19～0.98μg间有良好的线性关系(r=0.9997);平均回收率为99.9%,RSD为0.9%(n=6)。结论:方法简便、结果准确、重复性好,可作为该制剂的质量控制标准。Objective To establish a method for quality control of Tongjing Pills. Methods The Radix angelicae sinensis, Fructus evodiae were identified by TLC,the content of icariin was determined by HPLC. Results the spots in TLC were fairly clear,the linear range of icariin was 0.19～0.98μg （r=0.9997）;The average recovery was 99.9% with RSD 0.9%（n=6）. Conclusion This method is simple, accurate and repeatab：l：ty .It can be used for the quality control of tongjing pills.

关 键 词：痛经丸 薄层色谱法 淫羊藿苷 高效海相色谱法 

分 类 号：R927.2[医药卫生—药学]