GC-MS与直观推导式演进特征投影法分析青蒿挥发油化学成分  被引量:1

Analysis of Chemical Constituents of the Volatile Oil from Artemisia annua L. by GC/MS and Heuristic Evolving Latent Projection

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作  者:徐新建[1] 宋海[1] 朱小荣[1] 薛国庆[1] 安红刚 吴冬青[1] 

机构地区:[1]河西学院化学系西部资源环境化学重点实验室,甘肃张掖734000

出  处:《精细化工》2008年第12期1194-1197,共4页Fine Chemicals

基  金:西部资源环境化学重点实验室面上项目(XZ0705);甘肃省教育厅资助项目(0709B-02)~~

摘  要:用水蒸气蒸馏法从青蒿中提取挥发油。用气相色谱-质谱联用法进行了检测,再通过直观推导式演进特征投影(HELP)法对产生的二维色谱质谱数据进行了解析,得到各组分的纯色谱和质谱,对其化学成分进行了鉴定,用归一法计算了各组分的相对质量分数。分离得51个化学组分峰,并确定出其中43个化学成分,占挥发油总量的98.9。青蒿挥发油主要成分为w(Bisabolol)=23.47,w(Bisabolol oxide B)=11.31,w(Trans-Nerolidol)=10.04,w(Bisabolol oxide A)=6.27等。The volatile oil was extracted from Artemisia annua L. by steam distillation. The components of the volatile oil were separated and identified by GC - MS and heuristic evolving latent projection (HELP) method. The relative content of each component was determined by area normalization. Fifty-one components were separated, among which forty-three components were identified, accounting for about 98.9% of the total volatile oil. The main components are bisabolol(23.47% ) ,bisabolol oxide B (11.31%) ,trans-nerolidol( 10.04% ) and bisabolol oxide A(6.27%).

关 键 词:青蒿 挥发油 GC-MS 直观推导式演进特征投影法 中药现代化技术 

分 类 号:R284.1[医药卫生—中药学]

 

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