Synthesis and Characterization of NASICON Nanoparticles by Sol-gel Method  

作　　者：WANG Biao LIANG Xi-shuang LIU Feng-min ZHONG Tie-gang ZHAO Chun LU Ge-yu QUAN Bao-fu 

机构地区：[1]State Key Laboratory on Integrated Optoelectronics, College of Electronic Science and Engineering, Jilin University, Changchun 130012, P. R. China

出　　处：《Chemical Research in Chinese Universities》2009年第1期13-16,共4页高等学校化学研究（英文版）

基　　金：Supported by the Major International Collaborative Project of the National Natural Science Foundation of China(No. 60574096);the Distinguished Young Scholars(No.60625301).

摘　　要：Na superionic conductor（NASICON） nanoparticles were synthesized by a modified sol-gel method and sintered at a temperature range of 800--1000℃. The performance of the samples was characterized by the analysis methods of X-ray diffraction（XRD）, Fourier transform infrared spectroscopy（FTIR）, and transmission electron microscopy（TEM） as well as conductivity measurement. Compared with those sintered at other temperatures, the NASICON material sintered at 900 ℃ had the best crystalline structure and higher conductivity.Na superionic conductor（NASICON） nanoparticles were synthesized by a modified sol-gel method and sintered at a temperature range of 800--1000℃. The performance of the samples was characterized by the analysis methods of X-ray diffraction（XRD）, Fourier transform infrared spectroscopy（FTIR）, and transmission electron microscopy（TEM） as well as conductivity measurement. Compared with those sintered at other temperatures, the NASICON material sintered at 900 ℃ had the best crystalline structure and higher conductivity.

关 键 词：Na superionic conductor（NASICON） NANOPARTICLES Sol-gel method 

分 类 号：TN304.1[电子电信—物理电子学]