气相色谱法定量分析乙二醇单丁醚  

Quantitative determination of ethylene glycol monobutyl ether by gas chromatography

作　　者：朱京科[1] 潘水泉[1] 骆有寿[1] 朱京平[2] 

机构地区：[1]浙江大学化工系二次资源实验室,杭州310027 [2]杭州大学中心实验室,杭州310012

出　　处：《分析仪器》1998年第2期55-56,共2页Analytical Instrumentation

摘　　要：在装填聚二乙二醇丁二酸酯涂渍的硅烷化102白色担体的不锈钢柱上，成功地分离了反应液中的产品乙二醇单丁醚、副产品二乙二醇单丁醚、催化剂和溶剂各组分。分离在程序升温条件下进行。使用的检测器为热导检测器，以外标法定量分析乙二醇单丁醚和二乙二醇单丁醚，相对误差小于2．5％。篍thylene glycol monobutyl ether, by-product diethylene glycol ether and catalyst in reaction mixture wereseparated by gas chromatography on a stainless column packed with silanized 102 white support anted with polydiethyleneglycol succinate. The separation was performed under programmed temperature，The ethylene glycol monobutyl ether and ether anddiethylene glycol mnobutyl ether were detected by thermal conductivity detector.The external standard was used forquantitative analysis，The relative error was less than 2.5%

关 键 词：气相色谱 乙二醇单丁醚 定量分析 

分 类 号：O623.42[理学—有机化学] O623.423[理学—化学]