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作 者:陈卫明[1,2] 邓天龙[1,3] 张勤[2] 李庆霞[2]
机构地区:[1]成都理工大学材料与化学化工学院,四川成都610059 [2]中国地质科学院地球物理地球化学勘查研究所,河北廊坊065000 [3]中国科学院青海盐湖研究所,青海西宁810008
出 处:《岩矿测试》2009年第2期151-156,共6页Rock and Mineral Analysis
基 金:国家自然科学基金项目资助(40573044);四川省应用基础研究基金项目资助(05JY029-089-1);中央级公益性科研院所基本科研业务费专项资金资助(AS2007J5)
摘 要:文章总结了近年来土壤中有机氯农药残留分析的样品前处理和测定方法的研究进展,重点阐述微波萃取法、加速溶剂萃取法、固相萃取法、固相微萃取法、基质固相分散萃取法、超临界流体萃取法等前处理技术及气相色谱技术、气相色谱-质谱联用技术等在土壤中有机氯农药残留分析中的应用,指出了未来的发展趋势。The danger of organochlorine pesticide residue (OCPs) for ecological environment and human health is obvious. In this paper, progresses on sample preparation and analytical techniques and methods for OCPs in soil samples were reviewed. The main contents of the paper include sample preparation techniques of microwave extraction (ME), accelerated solvent extraction (ASE), solid phase extraction (SPE), solid phase micro extraction (SPME), matrix solid-phase dispersion extraction (MSPDE), supercritical fluid extraction (SFE), and the analytical techniques of gas chromatography (GC) and gas chromatography-mass spectrometry (GC-MS). The new development trends on this research area in the future were also pointed out.
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