治疗胆石症蒙药苏斯-12中多种元素的ICP-AES法测定及分析  

Determination of Trace Elements in Mongolian Medicine Susi-12 Curing Cholecystitis and Gallstone Disease by ICP-AES

作　　者：额尔登桑[1] 杭盖巴特尔 巴图[1] 段毅文[1] 

机构地区：[1]内蒙古师范大学化学与环境科学学院,内蒙古呼和浩特010022 [2]内蒙古中蒙医医院,内蒙古呼和浩特010022

出　　处：《光谱学与光谱分析》2009年第4期1108-1111,共4页Spectroscopy and Spectral Analysis

基　　金：内蒙古自治区自然科学基金项目(200408020216)资助

摘　　要：通过分析治疗胆囊炎、胆石症的蒙药苏斯—12中微量元素含量,探讨蒙药苏斯—12的药效与微量元素含量的关系。应用高压密封微波消解、电感耦合等离子体原子发射光谱法(ICP-AES)对蒙药苏斯—12进行微量元素含量分析。在蒙药的配制及整体研究工作中发现它们含有多种氨基酸和丰富的微量元素,实验结果表明:苏斯—12中含有丰富的微量元素,尤其Ca,Al,Mg,Fe,Sr,Mn,Zn,Cu等元素的含量比较高,而Pb,Cd,As等元素含量相对低,都低于国家限定值。加标回收率在94.63%～106.40%之间,相对标准偏差RSD≤3.35%,检出限在≤0.009μg·L-1。蒙药苏斯—12有效控制和治疗胆囊炎、胆石症,总有效率达91.2%和100%,蒙药苏斯—12中的微量元素与药效之间有密切的关系。Trace elements in Mongolian medicine Susi-12 for eholecystitis and gallstones were analyzed in order to discuss the relation between Susi-12＇s drug action and the trace elements. The analysis was carried out using the pressure seal microwave digestion and inductive coupled plasma atomic emission spectrometry （ICP-AES）. It was found that the medicine contained great amount of trace elements, especially human-body-needed trace elements, such as Ca, Al, Mg, Fe, Sr, Mn, Zn, Cu etc., whereas heavy metals are very little, e.g. the contents of Pb, Cb, As etc are below the country＇s limit. The recoveries of standard addition are in the range of 94. 63%-106. 40%. The relative standard deviation RSD≤3.35%, and detection limit is ≤0. 009 mg·L ^-1. It is concluded that Mongolian medicine Susi-12 can effectively control and cure cholecystitis and gallstones, and the effective rate reaches 91.2% to 100%. So the trace elements in Susi-12 must have a close connection with the drug action.

关 键 词：蒙药苏斯-12 微量元素、胆石症 ICP-AES 

分 类 号：O657.3[理学—分析化学]