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机构地区:[1]天津医科大学药学院/基础医学研究中心,天津300070
出 处:《中药材》2009年第4期515-517,共3页Journal of Chinese Medicinal Materials
摘 要:目的:对吊扬尘的化学成分进行分离和鉴定。方法:采用硅胶柱色谱、凝胶柱色谱、制备高效液相色谱等方法分离化合物,根据理化性质和波谱解析鉴定各化合物的结构。结果:从吊扬尘石油醚提取物中分离得到8个化合物:Buddlindeterpene B(1)、Buddledin B(2)、Buddledin C(3)、deacetyldihydrobuddledin A(4)、dihydrobuddledin C(5)、Suberosol B(6)、Gadain(7)、Hinokinin(8)。结论:化合物1、4~8为首次从该植物中分离得到。Objective: To study the chemical constituents of Rhizome of Buddleia davidii. Methods: The chemical constituents were isolated by repeated column chromatography (Toyopearl HW-40C and HPLC) and their structures were elucidated on the basis of physico-chemical properties and spectroscopic features. Results: From the petroleum ether extract of the material, eight compounds were isolated. Their structures were identified as : Buddlindeterpene B ( 1 ), Buddledin B (2), Buddledin C (3), deacetyldihydrobuddledin A(4), dihydrobuddledin C(5), Suberosol B(6), Gadain (7) and Hinokinin (8). Conclusion: Compounds 1,4 -8 are isolated from B. davidii for the first time.
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