高效液相色谱法测定织物涂层整理剂中的甲醛含量  

DETERMINATION OF FORMALDEHYDE CONTENT IN TEXTILE COATING AGENTS BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY METHOD

作　　者：赵婷[1] 赵梅[1] 温正如[1] 许伟[2] 

机构地区：[1]浙江传化股份有限公司,浙江杭州311215 [2]陕西科技大学资源与环境学院,陕西西安710021

出　　处：《陕西科技大学学报（自然科学版）》2009年第2期69-72,共4页Journal of Shaanxi University of Science & Technology

摘　　要：对织物涂层整理剂中微量甲醛的高效液相色谱分析方法进行了系统研究，对衍生条件和色谱分离方法进行了探讨，实现了对涂层整理剂中微量甲醛的准确定量．该方法线性关系良好，回归方程为y=3．8929x＋10．123（r=0．99993），线性范围为8．0-400mg／kg，加标回收率在93．2％～106．6％范围，不同浓度样品相对标准偏差在1．6％～6．89／6之间．A high performance liquid chromatography method for determination of trace formaldehyde in textile coating agents was reformed in this paper. The derivation and HPLC conditions were optimized to obtain good test results. The calibration curve for formaldehyde gave good linearity. The linear regression equation was established as y=3. 892 9x＋10. 123, with linearity range from 8. 0-400 mg/kg and correlation coefficient of 0. 999 3. The recovery range was 93. 2%-106. 6%, and the relative standard derivation （RSD） for different concentration samples was found to be 1.6%-6.8%

关 键 词：高效液相色谱法 涂层整理剂 甲醛 

分 类 号：O657.72[理学—分析化学] TS107[理学—化学]