分子蒸馏技术纯化玫瑰精油工艺研究  

Study on Refining of Rose Oil with Molecular Distillation

作　　者：韩荣伟[1] 于忠娜[2] 陈勇[1] 乔磊[1] 

机构地区：[1]青岛农业大学食品科学与工程学院,青岛266109 [2]青岛农业大学海都学院,莱阳265200

出　　处：《香料香精化妆品》2009年第3期1-4,9,共5页Flavour Fragrance Cosmetics

基　　金：山东省重点科技攻关项目(31040113);济南市科委重点资助项目(20030297);山东省农业科技成果转化资金项目(200540)

摘　　要：超临界CO2萃取所得的玫瑰粗油含蜡质较高,影响品质,采用无毒、无害、高效的分子蒸馏技术对其进行脱蜡,避免了传统有机溶剂法对精油品质的破坏,精油得率可达20.6%。正交试验表明分子蒸馏法提纯玫瑰精油最佳工艺条件为:蒸馏压力3.0Pa、蒸馏温度110℃、物料流量2mL/min、刮膜转速480r/min。Rose oil extracted with supercritical CO2 fluid extraction has much more waxes which affected its quality. It was refined with molecular distillation, the way which is non-toxic, innocuous and high efficient, and also avoid being destroyed by the traditional organic solvent method. Yield of refined rose oil reached 20.6%. Orthogonal test showed that the optimal refining conditions were determined as distillation pressure 3.0 Pa, distillation temperature 110 ℃, feed rate of rose oil 2 mL/min and agitating speed 480 r/min.

关 键 词：分子蒸馏 玫瑰精油 正交试验 

分 类 号：TQ654[化学工程—精细化工]