有机磷农药及氨基甲酸酯类农药的GC和GC/MS谱库的建立  

Establishment of Chromatogram and Spectra Library of Organophosphorus Pesticides and Carbamate Pesticides in GC and GC/MS

作　　者：黄诚[1] 梁建平[1] 罗小铭[1] 吴惠刚[1] 周日东[1] 陈子龙[1] 卢丽明[1] 谭家颖[1] 

机构地区：[1]广东省中山市疾病预防控制中心,528403

出　　处：《职业与健康》2009年第15期1581-1583,共3页Occupation and Health

摘　　要：目的通过气相色谱法(GC)和气质联用法(GC/MS)实现对16种有机磷农药及8种氨基甲酸酯类农药的分析鉴定。方法通过分析农药标准选择合适的GC分离条件,从而建立各农药的色谱图库和质谱法(MS)库。结果各种农药在不同色谱条件均能达到较好的分离,分析时间在25min内,分析鉴定结果可信度高。结论3种检测方法配合使用,快速、准确,适用于多种农药残留及中毒分析。[ Objective] To identify the 16 kinds of organophosphorus pesticides and 8 kinds of carbamate pesticides with gas chromatography （GC） and GC/MS. [Methods]Through the analysis of pesticide standards, the suitable GC separation conditions were selected, which set up the pesticide chromatography and MS spectral library database. [Results] A variety of pesticides at different chromatographic conditions were able to achieve better separation within 25min, with high reliability. [Conclusion] The conjunction of 3 identification method is rapid, accurate and applicable to a wide range of analysis of pesticide residues and poisoning.

关 键 词：有机磷 氨基甲酸酯 GC/FPD GC/NPD GC/MS 

分 类 号：R595.4[医药卫生—内科学] R284.1[医药卫生—临床医学]