荧烷类压、热敏染料FH-101的合成  

Synthesis of Pressure thermal Sensitive Dye of Fluoran

作　　者：潘建林[1,2] 陶兰[1,2] 张华松[1,2] 顾一新[1,2] 李连武 

机构地区：[1]杭州师范学院化学系 [2]仙居粮油化工厂

出　　处：《精细化工》1998年第4期23-25,共3页Fine Chemicals

摘　　要：合成了显黑色的压、热敏染料３二乙基氨基７（２’氯苯胺基）荧烷，较佳的制备条件是：二苯甲酮衍生物与二苯胺衍生物的摩尔比为１∶１２，硫酸质量分数（Ｈ２ＳＯ４）为９０％，反应时间为２４ｈ，产物的收率达６２％。The pressure thermal sensitive dye of fluoran 3 diethylamino 7 (2' chloroanilino)fluoran(FH 101)was synthesized,some factors which affected the reactions were researched.The result showed that molar ratio of derivatives of benzophenone to diphenylamine was 1∶1.2,mass fraction of sulfuric acid was 90%,reaction time was 24h.And the yield was 62%.

关 键 词：荧烷 染料 压敏染料 热敏染料 FH-101 感光材料 

分 类 号：TQ618.97[化学工程—精细化工]