N-(2-羟基乙基)肉桂酰胺的合成工艺研究  

Studies on synthesis of N-(2-hydroxyethyl)cinnamamide

作　　者：修景会[1] 权迎春[1] 郑光浩[1] 关丽萍[1,2] 

机构地区：[1]延边大学药学院,吉林延吉133000 [2]延边大学长白山生物资源与功能分子教育部重点实验室,吉林延吉133002

出　　处：《化学试剂》2009年第8期663-663,666,共2页Chemical Reagents

摘　　要：以肉桂酸为起始原料,经一步反应制得标题化合物。投料比为肉桂酸∶氯甲酸甲酯∶乙醇胺=1∶1.08∶2。其结构经IR、1HNMR、MS等确证,产率75%。N-（2-Hydroxy ethyl）cinnamamide was synthesized by one-step reaction using cinnamic acid as the starting material.The molar ratio of cinnamic acid to methyl chloroformate,and ethanolamine was 1∶1.08∶2.The chemical structure of the target compound was confirmed by IR,^1HNMR and MS.The yield of the title compound was 75%.

关 键 词：N-(2-羟基乙基)肉桂酰胺 合成 

分 类 号：O623.73[理学—有机化学]