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作 者:罗艺萍[1,2] 赵兴堂[2] 羊晓东[2] 赵静峰[2] 李良[2]
机构地区:[1]思茅师范高等专科学校生命科学系,云南普洱665000 [2]云南大学教育部自然资源药物化学重点实验室,云南昆明650091
出 处:《云南化工》2009年第4期45-47,共3页Yunnan Chemical Technology
摘 要:细穗兔儿风Ainsliaea spicata干燥全草的95%工业乙醇提取物,用石油醚萃取,浓缩后上硅胶柱层析,V(石油醚)/V(乙酸乙酯)为60∶1洗脱,即得到其挥发油成分。用GC-MS联机手段进行分析,鉴定了15个化合物,并采用线性归一方法测定各化学成分的相对含量。Ainsliaea spicata belongs to Compositae Ainsliaea, it's whole plant is used in folk recipe. The dried powders of Ainsliaea spicata were extracted with 95 % EtOH in our study. Then EtOH was evaporated and the residue was extracted with Petroleum ether. The extract was chromatographed on a silica gel column, and was eluted with petroleum ether - ethyl acetate (60:1 ) . The volatile components were obtained in the first part. 15 eonstituents were identified, and their relative contents were determined by peak area normalization method in GC-MS.
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