切削液和机床排泄物中汞的测定-直接测汞法  

Direct Determination of Mercury in Cutting Fluid and Machining Process Waste Fluid

作　　者：余淑媛[1] 刘贤杰[1] 任聪[1] 陈向阳[1] 吴景武[1] 刘志红[1] 刘丽[1] 李辉[1] 王成云[1] 

机构地区：[1]深圳出入境检验检疫局

出　　处：《光谱实验室》2009年第4期955-958,共4页Chinese Journal of Spectroscopy Laboratory

基　　金：科技部十一五国家科技支撑计划课题(项目编号2006BAK10B03)

摘　　要：建立了直接进样测定切削液和机床排泄物中汞含量的无损分析方法。该方法准确度和精密度高,方法检出限可达0.07ng,回收率在87.3%—106.5%范围内,该方法解决了样品前处理过程中汞的损失问题,并大大缩短了汞的检测时间,用于切削液和机床排泄物中汞含量测定,结果满意。A new method for the determination of mercury in cutting fluid and machining process waste fluid by cold atomic absorption spectrometry coupled with direct sampling method was established.The caccuracy and precision of the direct determination method of mercury were reliable.The detection limit of the method was 0.07ng while the recovery was from 87.3% to 106.5%.This method solved the mercury losing problem in the handling process and reduced the analytical period obviously and could be applied to the direct determination of mercury in cutting fluid and machining process waste fluid with satisfactory results.

关 键 词：切削液 机床排泄物 汞 直接测汞法 

分 类 号：O657.31[理学—分析化学]