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机构地区:[1]中国科学技术大学应用化学系
出 处:《感光科学与光化学》1998年第3期193-196,共4页Photographic Science and Photochemistry
基 金:安徽省自然科学基金;国家自然科学基金
摘 要:1991年Iijima[1]在研究C60的同时,首次在高分辨透射电镜(HRTEM)下发现具有纳米尺寸的被称为纳米碳管(carbonnanotube)的中空的多层管状物.1992年Ebbesen等人[2]发现了大量合成这种纳米管的方法.这种新物质的出现...In this paper, the high resolution transmission electronic microscopy(HRTEM, resolution of 0.2 nm) is employed to observe the crystal structure of the developed silver filament from the nanometer sized silver halide emulsions. We carry out the research work on the “empty tube” and the “core thread” remaining in the tube after prolonged fixation. The results show that the thin string is a kind of polycrystal silver consisted of many crystalline grains, containing many microtwins and defects. There is no difference in the crystal structures between silver filaments and the core thread. Besides, according to our observation, the empty tube is another kind carbon nanotube made up of amorphous carbon. The reaction in the empty carbon tube may become a distinctive method to prepare the various thinner nanometer sized string.
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