对溴苯基烯丙基醚的催化合成研究  

The Synthesis of 4-Bromophenyl Allyl Ether by Catalyst

作　　者：周冬香[1] 李立[1] 刘润山[2] 

机构地区：[1]上海海洋大学食品学院,上海201306 [2]湖北省化学研究院,湖北武汉430074

出　　处：《广州化工》2009年第6期91-92,共2页GuangZhou Chemical Industry

摘　　要：在无机催化剂溴化纳存在下,通过对溴苯酚与氯丙烯反应,高收率的生成了对溴苯基烯丙基醚。研究了催化剂的用量,水醇比,反应时间对收率和质量的影响。通过FT-IR、1H-NMR、GC-MS等进行表征,证实了产物的纯度和催化剂的有效及工艺的可行性。4- Bromophenyl allyl ether was prepared by the reaction of 4- Bromo- phenol with allyl chloride in the presence of inorganic catalyst. The influence of the reaction time, the quantities of catalysts on the yield and quality were investigated. The structure and properties were characterized by FT - IR, ^1H - NMR, GC - MS. It attested that the outcome was very pure, the inorganic catalyst was effective and the process was feasible.

关 键 词：对溴苯基烯丙基醚 无机催化剂 对溴苯酚 氯丙烯 

分 类 号：TQ323.42[化学工程—合成树脂塑料工业] O643.36[理学—物理化学]