3,6-二碘代-9-(4-甲基苯基)咔唑的合成  

Synthesis of 3,6-diiodo-9-p-tolyl-9H-carbazole

作　　者：魏红玉[1] 赵睿新[2] 张鑫[1] 李奋强[1] 张昭[1] 

机构地区：[1]山西大学化学化工学院,山西太原030006 [2]山西财经大学环境经济系,山西太原030006

出　　处：《化学试剂》2009年第9期745-746,共2页Chemical Reagents

摘　　要：以咔唑为原料,通过Ullmann反应、碘代反应合成标题化合物,并对反应条件进行了优化选择。所得产物的结构经红外光谱、核磁共振氢谱表征。3,6-Diiodo-9-p-tolyl-9H-carbazole used as the intermediate of organic electroluminescent material was synthesized via Ullmann reaction followed by iodination on carbazole.The optimum reaction conditions were determined.The structure of the target compounds was confirmed by IR and ^1HNMR.

关 键 词：9-(4-甲基苯基)咔唑 碘代 3 6-二碘代-9-(4-甲基苯基)咔唑 有机合成 

分 类 号：O621.3[理学—有机化学]