2,6-二叠氮甲基-1,7-二叠氮庚烷的合成及表征  

Synthesis and characterization of 2,6-bis(azidomethyl)-1,7-diazido heptane compound

作　　者：唐光诗[1] 王鹏慧[1] 李丽[1] 

机构地区：[1]北京化工大学理学院,北京100029

出　　处：《化学试剂》2009年第10期843-845,共3页Chemical Reagents

摘　　要：使用传统的合成手段,通过官能团的替换,由简单分子高产率地合成了具有高度活性的标题化合物。每一步的产物结构由1HNMR和13CNMR确证。对不同的取代基对邻近氢化学位移的影响作了对比和初步的分析。The highly active four-functional compound 2,6-bis（azidomethyl）-1,7-diazido heptane was synthesized with a high yield,according to the traditional synthetic method realized through the functional group replacement.The structure of the product was confirmed by 1HNMR and 13CNMR.A discussion relating to the influence of different substitutes on chemical shift of adjacent hydrogen was made.

关 键 词：四叠氮化合物 合成 应用 

分 类 号：O622[理学—有机化学]