氧化型染发剂的有机成分分析及多种染料中间体的测定  

Analysis of organic components in oxidation hair dye and determination of multilevel dyestuff intermediate

作　　者：董巧红[1] 陈艳美[2] 石金娥[1] 于海玲[3] 

机构地区：[1]吉林省产品质量监督检验院,长春130022 [2]吉林工商学院,长春130025 [3]吉林农业大学,长春130118

出　　处：《中国卫生检验杂志》2009年第11期2533-2535,共3页Chinese Journal of Health Laboratory Technology

摘　　要：目的:依据《化妆品卫生规范》要求,建立8种指定染料中间体的测定方法,并对氧化型染发剂的主要成分进行监测。方法:样品经乙醚超声提取,离心过滤后分别用GC(定量)、GC/MS(定性),并采用GC/MS对检测结果进行验证。结果:建立了染发剂中8种指定染料中间体的气相色谱分析方法,同时对市售6种染发剂成分进行了定性分析,明确了染发剂中两剂各自的成分及含量。结论:该方法操作简便、灵敏度高、检测限低,线性范围合理,可满足氧化型染发剂的日常检测。同时,还定性分析了染发剂中两剂的主要成分,有利于指导消费者对染发剂的正确认识,有助于染发剂和对人体健康的研究。Objective：To monitor primary components of oxidation hair dye and confirm eight determinate methods of appointed dyestuff intermediate based on Health Criterion of Toiletry.Methods：Samples were disposed by ultrasonic extraction of aether.GC and GC/MS were used after centrifugal abruption while GC/MS was used to validate the outcome.Results：Eight gas chromatography methods of dyestuff intermediate and qualitative analysis of six hair dyes on sale were achieved.Conclusion：The method which is simple,sensitive and of low limitation and reasonable can meet the daily determination of oxidation hair dyes.The qualitative analysis of two primary components in hair dyes is contributed to guiding consumer and research on hair dyes and health.

关 键 词：氧化型染发剂 染料中间体 有机成分 分析 

分 类 号：TQ658[化学工程—精细化工]