3-氨基-4-氯苯腈的合成及表征  

Synthesis and Identification of 3 Amino 4 Chloro Benzonitrile

作　　者：王明星[1] 宋溪明[1] 常晓红 

机构地区：[1]辽宁大学化学科学与工程学院

出　　处：《辽宁大学学报（自然科学版）》1998年第4期373-375,共3页Journal of Liaoning University：Natural Sciences Edition

摘　　要：本文采用对氯苯甲醛为起始原料制得对氯苯腈，经硝化、还原得标题化合物．并对其进行了物化常数、ＩＲ、１ＨＮＭＲ、ＭＳ及元素分析等检测，结果表明：结构正确，该合成路线工艺合理，具有实用开发价值．amino 4 chloro benzonitrile(TMS) was synthesized from 4 chloro benzaldehyde through nitrification and reduction, and its physical and chemical constants were determined with the method of IR, MS, HNMS and element analysis. The results show that the structure is correct, the synthetic route is reasonable, and this synthetic method is of practical value for development.

关 键 词：氯苯腈 合成 硝化 氨基氯苯腈 工艺 表征 

分 类 号：O625.6[理学—有机化学] TQ246.7[理学—化学]