微波辐射合成5-羧基-3-氨基-1,2,4-三氮唑  

Synthesis of 5-acid-3-amino-1,2,4-triazole under microwave irradiation

作　　者：何冰晶[1] 何灵官[1] 

机构地区：[1]台州学院医药化工学院,浙江临海317000

出　　处：《化学工程师》2009年第12期12-13,共2页Chemical Engineer

摘　　要：本文在微波辐射条件下合成5-羧基-3-氨基-1,2,4-三氮唑,产物结构通过IR,1HNMR进行了表征。微波反应条件下的反应速度是常规条件下反应速度的66倍,并且产率相当。5-Acid- 3-amino-l,2,4-triazole was synthesized under microwave irradiation. The structure of new compound was confirmed by IR and-^1H NMR. Compared with the conventional synthesis, the reaction rate was up to about 66 times faster under microwave irradiation, and the yield was comparable.

关 键 词：微波辐射 5-羧基-3-氨基-1 2 4-三氮唑 合成 

分 类 号：O626[理学—有机化学]