腐霉利·百菌清复合烟剂的气相色谱分析  

Analytical Method of Procymidone and Chlorothalonil in Smoke Generator By Gas Chromatography

作　　者：夏雨[1] 吴亚玉[1] 张耀中[1] 孙敏[1] 姜士聚[1] 

机构地区：[1]山东省农药检定所

出　　处：《农药科学与管理》1998年第A05期5-6,共2页Pesticide Science and Administration

摘　　要：本文介绍选用５％ＸＥ－６０，１ｍ×３ｍｍ（ｉ．ｄ）玻璃柱，以正二十八碳烷为内标物，在１９５℃柱温下对腐霉利·百菌清烟剂中有效成分腐霉利和百菌清同时进行气相色谱分析。百菌清的标准偏差为０．１３６，变异系数为１．３０％，回收率为９９．２７％，线性相关系数为０．９９９９；腐霉利的标准偏差为０．０７０，变异系数为０．６２６％，回收率为９９．７８％，线性相关系数为０．９９９９。This paper reported a specific quantitative analysis method of procymidone and chlorothalonil in smoke generator by using gas-liquid chromatography with glass chromatographic column packed with 5% XE-60 and octacosane as internal standard. The condition was that the column temperature was 195℃ and the FID detector was used.The standard deviation 、 coefficient of variation 、linear correlation, and the average recovery of chlorothalonil were 0.136,1.30%,0.9999 and 99.27% respectively. Those of procymidone were 0.070,0.626%,0.9999 and 99.78% respectively.

关 键 词：腐霉利 百菌清 杀菌剂 气相色谱分析 复合烟剂 

分 类 号：TQ450.7[化学工程—农药化工] S482.2[农业科学—农药学]