微波辐射下合成N-芳基和N-杂环取代氰乙酰胺  

THE SYNTHESIS OF N SUBSTITUTED ARYL AND HETEROCYCLE CYANOAMIDES UNDER MICROWAVE RADIATION

作　　者：邵建国[1,2] 王佩玉[1,2] 郑鸣 钟琦[1,2] 

机构地区：[1]扬州大学师范学院化学化工系 [2]扬州大学医学院基础部

出　　处：《扬州大学学报（自然科学版）》1998年第2期17-20,共4页Journal of Yangzhou University：Natural Science Edition

基　　金：江苏省教委自然科学基金

摘　　要：在微波辐射下合成Ｎ芳基和Ｎ杂环取代氰乙酰胺，产率达８３％～９５％．反应是在经过改进的容器中进行的，容器置于频率为２４５０ＭＨｚ的微波炉中，常压下６～１０ｍｉｎ即可完成反应，反应速度快，后处理方便．N substituted aryl and heterocycle cyanoamides are synthesized under microwave radiation, with the yields 83%～95%. The reaction is carried out in an improved container which is put into a microwave oven at 2 450 MHz. The reaction can be finished within 6￣10 min under normal pressure. The products can also be very conveniently treated.

关 键 词：微波辐射 氰乙酰胺 合成 芳基 杂环取代基 

分 类 号：O625.632[理学—有机化学] O626[理学—化学]